Use a pipette with a filler to to measure out a volume of alkaliput the alkali into a flask with a few drops of indicator and swirl the flaskUsing a funnel, fill a burette with some acid of a known concentration then place the flask containing hte alkali under the buretteTake a reading of the volume of acid in the burette by measuring at the bottom of the meniscuscomplete a rough titration by adding the acid to the alkali a bit at a time, giving the flask a regular swirlContinue until the indicator changes colour. this happens when the alkali has been fully neutralisedrecord the volume of acid left in the bueretteCalculate the amount of acid needed to neutralise the alkali by subtracting the initial reading of acid in the burette from the final reading of acid in the burette Now do an accurate titrationUse the qauntity of acid you found doing the rough titration and add all but 2cm of itadd the rest of the acid drop by drop very slowly and spot exactly where the indicator changes colourcalculate the volume of acid used to neutralise the acidrepeat the accurate titration until you get at least 3 concordant resultscalculate the mean volume of acid that was needed to neutralise the acid. Only use concordant results