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Chemistry
Required Practicals (C)
Making soluble salts
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Cards (7)
Equipment for the first stage
beaker
gauze
tripod
heatproof mat
Stage one
start with a
fixed volume
of a
dilute acid
this is the
limiting reactant
there should not be any acid remaining at the end
gently heat the acid until it is almost boiling
do not let it boil
Stage 2
use a spatula to add small amounts of the oxide (
reactant
) to the acid
stir the solution using a
glass rod
the oxide will react and seem to disappear
continue adding oxide if the solution continues to be clear
stop adding the powder once it starts to remain after being stirred
Once the powder stops dissolving, all of the
acid
has reacted and the solution is now
neutral
Stage 3
remove the
unreacted
powder
it can be filtered out using
filter paper
as it is an
insoluble
solid
it is filtered using a
filter funnel
and filter paper
Stage 4
the solution is placed in an
evaporating basin
this is heated gently over a
beaker
of boiling water
leave this until about half the solution has evaporated and small
crystals
are visible
leave the solution in a cool place
Stage 5
after
24 hours
, once the
crystals
have formed, scrape them on a paper towel
gently pat them dry
what's left are pure, dry crystals of the salt