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Edexcel A-Level Chemistry
Core Practicals
CP2 Preparation of a Standard Solution and Titration
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What is a standard solution?
Solution with known concentration
The accurate concentration of a standard solution is crucial for precise
stoichiometric
When preparing a standard solution, the first step is to dissolve the solute in water.
False
Steps for preparing a standard solution from a solid solute
1️⃣ Weigh the solute accurately using a balance
2️⃣ Dissolve the solute in a solvent
3️⃣ Transfer the solution to a volumetric flask
4️⃣ Add solvent to the graduation mark
To prepare a standard solution from a solid solute, a volumetric
flask
Match the type of standard solution with its preparation method:
Solid Solute ↔️ Weigh, dissolve, transfer to flask
Liquid Solute ↔️ Measure volume, dilute in flask
Dilution from Stock ↔️ Dilute stock solution
The formula to calculate the mass needed to prepare a standard solution is Mass = Molarity × Volume × Molar
Mass
The first step in weighing the solute for a standard solution is to tare the balance.
True
Match the weighing procedure with its pros and cons:
With Weighing Boat ↔️ Keeps balance clean, requires extra container
Without Weighing Boat ↔️ No extra container, can spill solute easily
When using a weighing boat, you must
tare
the balance after placing the weighing boat on it.
True
Match the procedure with its pros and cons:
Taring with Weighing Boat ↔️ Keeps the balance clean, requires an extra container
Taring without Weighing Boat ↔️ Simplifies process, may contaminate the balance
Stoichiometric calculations in titrations rely on the accurate
concentration
of standard solutions.
True
The formula to calculate the mass needed to prepare a standard solution is Mass = Molarity × Volume × Molar
Mass
What does the volume in the mass formula refer to?
Volume of the solution
To prepare 500 mL of a 0.1 mol/L NaOH solution, you need to weigh out
2 grams
of solid NaOH.
True
When using a weighing boat, tare the balance after placing the weighing
boat
Taring with a weighing boat simplifies the process and uses fewer materials.
False
Taring with a weighing boat keeps the balance
clean
Why is accurate weighing crucial in preparing standard solutions?
Reliable titration results
To prepare 500 mL of a 0.1 M NaOH solution,
2 grams
of solid NaOH are required.
True
Rinsing the beaker with distilled water ensures all the dissolved
solute
is transferred.
Why is using a volumetric flask with a calibrated volume mark essential?
Accurate standard solution
When approaching the calibration mark, it is important to avoid
overfilling
the flask.
True
Standard solutions are crucial for accurate stoichiometric
calculations
The formula "Mass = Molarity × Volume ×
Molar Mass
" is used to calculate the mass needed to prepare a standard solution.
True
Molarity is measured in moles per
liter
Ensure the balance is clean, level, and
calibrated
Taring the balance with a weighing boat requires pressing the "
tare
" button to set the display to zero.
True
Using distilled water ensures the solution is free of any
impurities
A volumetric flask with a calibrated volume mark is essential for preparing an accurate
standard solution
.
True
Overfilling the volumetric flask should be corrected by carefully adjusting the water level with a
dropper
.
True
Steps to set up a titration apparatus
1️⃣ Secure the burette in a clamp
2️⃣ Place the receiving flask on a stirrer
3️⃣ Add a few drops of indicator
4️⃣ Fill the burette with titrant
Add a few drops of the appropriate
indicator
to the analyte solution in the receiving flask.
The receiving flask in a titration setup should always be placed on a magnetic stirrer plate if available.
True
What should you ensure about the burette stopcock before starting titrant delivery?
It is closed
Accurate and precise setup of a titration apparatus is crucial for obtaining
reliable
results.
True
What part of the standard solution in the burette must you adjust to the zero or starting mark?
Meniscus
The accurate concentration of a standard solution is crucial for precise
stoichiometric
calculations during titrations.
What is the formula for calculating the mass needed to prepare a standard solution?
Mass = Molarity \times Volume \times Molar \ Mass</latex>
How many grams of NaOH are needed to prepare 500 mL of a 0.1 mol/L solution?
2 grams
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