Measure of the molar volume of a gas
1. Set up the apparatus to capture and measure gas evolved from a reaction in the boiling tube
2. Place 30 cm3 of 1 mol dm−3 ethanoic acid in the boiling tube
3. Place approximately 0.05 g of calcium carbonate in a test tube. Weigh the test tube and its contents accurately
4. Remove the bung from the boiling tube and tip the calcium carbonate into the boiling tube. Quickly replace the bung in the boiling tube
5. Once the reaction is over, measure the volume of gas produced
6. Reweigh the test tube that contained the calcium carbonate
7. Repeat the experiment six more times, increasing the mass of calcium carbonate by about 0.05 g each time. Do not exceed 0.40 g of calcium carbonate